1,1-双(P-氯苯基)-2-氯乙烯合成路线 （共 30 条）
反应条件
tris(2,2'-bipyridyl-N,N')cobalt(II) diperchlorate in N-dodecane; water
T=30°C; Dehalogenation; 3 h; Electrolysis-1 V vs. Ag/AgBr; Further byproducts given;
参考文献
Schweizer, Silvia; Rusling, James F.; Huang, Qingdong
Chemosphere, 1994 , vol. 28, # 5 p. 961 - 970
反应条件
1: diethyl ether
2: concentrated H2SO4
View Scheme
参考文献
Pepper; Kulka
Journal of the American Chemical Society, 1950 , vol. 72, p. 1417
反应条件
1: diethyl ether
2: concentrated H2SO4
View Scheme
参考文献
Pepper; Kulka
Journal of the American Chemical Society, 1950 , vol. 72, p. 1417
反应条件
1: isopropyl alcohol
2: H2SO4 / 30 °C / zuletzt bei 60grad
3: NaOH
View Scheme
参考文献
Haller et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1591,1599
反应条件
1: n-BuLi, HMDS / tetrahydrofuran; hexane / 1.) -78 deg C, 10 min, 2.) -78 deg C to r.t., 30 min
2: 1.) n-BuLi, 2.) HCl / 1.) THF, hexane, -90 deg C, 5 min, 2.) EtOH, -90 deg C
View Scheme
参考文献
Mouries, Virginie; Waschbuesch, Rachel; Carran, John; Savignac, Philippe
Synthesis, 1998 , # 3 p. 271 - 274
反应条件
CaO
T=20°C; Decomposition; 12 h; Further byproducts given;
参考文献
Hall, Annegret K.; Harrowfield, Jack M.; Hart, Reinhold J.; Mccormicr, Paul G.
Environmental Science and Technology, 1996 , vol. 30, # 12 p. 3401 - 3407
反应条件
in hexane
Irradiation;
参考文献
Kerner,I. et al.
Tetrahedron, 1972 , vol. 28, p. 1575 - 1578
反应条件
in N-dodecane; water
T=30°C; Dehalogenation; 3 h; Electrolysis-2 V vs. Ag/AgBr; Further byproducts given;
参考文献
Schweizer, Silvia; Rusling, James F.; Huang, Qingdong
Chemosphere, 1994 , vol. 28, # 5 p. 961 - 970
反应条件
in N-dodecane; water
T=30°C; Dehalogenation; 3 h; Electrolysis-2.3 V vs. Ag/AgBr; Further byproducts given;
参考文献
Schweizer, Silvia; Rusling, James F.; Huang, Qingdong
Chemosphere, 1994 , vol. 28, # 5 p. 961 - 970
反应条件
Triton X-114; sodium hydroxide; iron in water
T=20°C; Dehalogenation; 480 h; Kinetics; Further Variations:also without surfactant and iron;
参考文献
Sayles, Gregory D.; You, Guanrong; Wang, Maoxiu; Kupferle, Margaret J.
Environmental Science and Technology, 1997 , vol. 31, # 12 p. 3448 - 3454
