2-苯基-4-[3H]喹唑啉酮合成路线 (共 178 条)
反应条件
palladium diacetate; diphenylphosphinobenzene-3-sulfonic acid sodium salt in water-d2 T=120°C; 16 h; sealed tubeInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 16 p. 7046 - 7051
反应条件
palladium diacetate; diphenylphosphinobenzene-3-sulfonic acid sodium salt in water T=120°C; 16 h; sealed tubeInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 16 p. 7046 - 7051
反应条件
1: triethylamine / dichloromethane / 0 °C 2: ammonium hydroxide / isopropyl alcohol / 10 h / 90 °C / |Sealed tube 3: potassium tert-butylate / tetrahydrofuran / 0.17 h / 40 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 35 p. 5908 - 5912
反应条件
1: triethylamine / dichloromethane / 0 °C 2: ammonium hydroxide / isopropyl alcohol / 10 h / 90 °C / |Sealed tube 3: potassium tert-butylate / tetrahydrofuran / 0.17 h / 40 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 35 p. 5908 - 5912
反应条件
1: ammonium hydroxide / isopropyl alcohol / 10 h / 90 °C / |Sealed tube 2: potassium tert-butylate / tetrahydrofuran / 0.17 h / 40 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 35 p. 5908 - 5912
反应条件
1: N-chloro-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C / |Inert atmosphere 2: triethylamine / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / |Inert atmosphere 3: oxygen; caesium carbonate / dimethyl sulfoxide / 2.5 h / 100 °C / 760.05 Torr View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 36 p. 6003 - 6007
反应条件
1: triethylamine / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / |Inert atmosphere 2: oxygen; caesium carbonate / dimethyl sulfoxide / 2.5 h / 100 °C / 760.05 Torr View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 36 p. 6003 - 6007
反应条件
water T=200°C; 12 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 42, # 16 p. 4481 - 4492
反应条件
water T=200°C; 12 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 42, # 16 p. 4481 - 4492
反应条件
in N,N-dimethyl-formamide 9 h; Heating;
参考文献
Tetrahedron, , vol. 42, # 5 p. 1449 - 1460