2-苯基-4-[3H]喹唑啉酮合成路线 （共 178 条）
反应条件
dimethyl sulfoxide 1.) r.t., 20 h; 2.) 100 deg C, 6 h;
参考文献
Journal of the Indian Chemical Society, , vol. 65, p. 136 - 137
反应条件
in toluene T=110°C; 96 h;
参考文献
Heterocycles, , vol. 45, # 7 p. 1309 - 1318
反应条件
in ethanol 4 h; Heating;
参考文献
Russian Chemical Bulletin, , vol. 47, # 12 p. 2441 - 2444
反应条件
1: acetic anhydride / 2 h / Heating 2: NH4OH / ethanol / Heating View Scheme
参考文献
Heterocyclic Communications, , vol. 10, # 4-5 p. 325 - 330
反应条件
1: PCl5 / benzene / 50 - 60 °C 2: 2.) TiCl4, 3.) 20percent aq. HCl View Scheme
参考文献
Polish Journal of Chemistry, , vol. 68, # 3 p. 489 - 498
反应条件
1: K2CO3 / diethyl ether / 2 h / Heating 2: aq. HCl, KCl / dioxane / 50 °C / var. HCl concentration; other 2-(substituted benzamido)benzonitriles View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 11 p. 2171 - 2174
反应条件
1: thionyl chloride / 1,2-dichloro-ethane / 4 h / Reflux 2: ammonia / 1,2-dichloro-ethane / 20 °C 3: palladium 10 on activated carbon; hydrogen / methanol 4: sodium hydrogensulfite / N,N-dimethyl acetamide / 3 h / 150 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 7 p. 2709 - 2721
反应条件
1: palladium 10 on activated carbon; hydrogen / methanol 2: sodium hydrogensulfite / N,N-dimethyl acetamide / 3 h / 150 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 7 p. 2709 - 2721
反应条件
1: ammonia / 1,2-dichloro-ethane / 20 °C 2: palladium 10 on activated carbon; hydrogen / methanol 3: sodium hydrogensulfite / N,N-dimethyl acetamide / 3 h / 150 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 7 p. 2709 - 2721
反应条件
1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0 - 20 °C / Inert atmosphere 1.2: Inert atmosphere; Cooling with ice 2.1: palladium diacetate; acetic acid; copper(II) oxide / 4 h / 110 °C / 760.05 Torr 3.1: palladium diacetate; acetic acid; copper(II) oxide / 23 h / 110 °C / 760.05 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 15 p. 6362 - 6366
