2-苯基-4-[3H]喹唑啉酮合成路线 (共 178 条)
反应条件
1: With caesium carbonate; L-proline in N,N-dimethyl-formamide T=20°C; 0.5 h; Inert atmosphere; 2: With copper(l) iodide in N,N-dimethyl-formamide T=20 - 80°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , # 47 p. 6333 - 6335
反应条件
1: With caesium carbonate; L-proline in N,N-dimethyl-formamide T=20°C; 0.5 h; Inert atmosphere; 2: With copper(l) iodide in N,N-dimethyl-formamide T=20 - 80°C; 16 h; Inert atmosphere;
参考文献
Chemical Communications, , # 47 p. 6333 - 6335
反应条件
in dimethyl sulfoxide T=100°C; P=760.051 Torr; 2 h;
参考文献
Organic Letters, , vol. 15, # 11 p. 2842 - 2845
反应条件
oxygen; caesium carbonate in dimethyl sulfoxide T=100°C; P=760.051 Torr; 2.5 h; Reagent/catalystSolventTemperature;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 36 p. 6003 - 6007
反应条件
oxygen; potassium carbonate; copper(I) bromide in dimethyl sulfoxide T=110°C; Ullmann-type condensation; 8 h;
参考文献
Organic Letters, , vol. 13, # 6 p. 1274 - 1277
反应条件
FeCl3·6H2O; sulfur in neat (no solvent) T=140°C; 24 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 24 p. 6218 - 6221
反应条件
urea-hydrogen peroxide; potassium carbonate in water; acetone 2 h; Heating;
参考文献
Synthetic Communications, , vol. 27, # 12 p. 2065 - 2068
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20°C; 10 h; Inert atmosphereSealed tube;
参考文献
Applied Organometallic Chemistry, , vol. 26, # 11 p. 576 - 582,7
反应条件
oxygen; potassium carbonate; copper(I) bromide in dimethyl sulfoxide T=110°C; Ullmann-type condensation; 8 h;
参考文献
Organic Letters, , vol. 13, # 6 p. 1274 - 1277
反应条件
potassium phosphate; oxygen in N,N-dimethyl-formamide T=100°C; P=760.051 Torr; 1.5 h; Reagent/catalystSolventTemperature;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 36 p. 6003 - 6007