1-(4-硝基苯基)吡咯烷合成路线 (共 35 条)
反应条件
in tetrahydrofuran T=50°C; P=9000720 Torr; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 1 p. 42 - 49
Chemistry Letters, , p. 1187 - 1190
反应条件
1: 4-fluoro-nitro-benzene With cesium fluoride in N,N-dimethyl-formamide 0.166667 h; Inert atmosphere; 2: 1-(trimethylsilyl)pyrrolidine in N,N-dimethyl-formamide T=60°C; 6 h;
参考文献
US2012/142937 A1, ;
Page/Page column 5-6 ;
反应条件
in tetrahydrofuran T=50°C; P=4500360 Torr; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 1 p. 42 - 49
Chemistry Letters, , p. 1187 - 1190
反应条件
in tetrahydrofuran T=50°C; P=6375510 Torr; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 1 p. 42 - 49
反应条件
potassium hydroxide; air; Cd(CH3COO)2*2H2O; ethylene glycol in dimethyl sulfoxide T=85°C; 2.5 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 350, # 3 p. 395 - 398
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yield given;
参考文献
Synthesis, , # 1 p. 74 - 79
反应条件
in tetrahydrofuran T=80°C; P=5625450 Torr; 20 h;
参考文献
Chemistry Letters, , # 2 p. 359 - 362
Bulletin of the Chemical Society of Japan, , vol. 68, # 9 p. 2717 - 2726
反应条件
anhydrous sodium hydrogen carbonate in 1,4-dioxane; water
反应条件
cesium fluoride in N,N-dimethyl-formamide T=60°C; 6 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 4 p. 1151 - 1154
反应条件
dimethylsulfide borane complex in tetrahydrofuran 9 h; Heating;
参考文献
Synthesis, , # 12 p. 985 - 988