sodium t-butanolate in tert-butyl alcohol T=20 - 25°C; 3.5 h; Large scale;
参考文献
Bannister, Robin M.; Brookes, Michael H.; Evans, Graham R.; Katz, Ruth B.; Tyrrell, Nicholas D.
Organic Process Research and Development, 2000 , vol. 4, # 6 p. 467 - 472
1: potassium hydroxide / ethanol; water / |Large scale 2: ethyl acetate / 2 h / 60 - 65 °C / |Large scale 3: 3-nitro-phenyl boronic acid / anhydrous xylene / 24 h / 40 °C / |Reflux 4: dimethylsulfide borane complex / tetrahydrofuran / 16 h / 0 - 25 °C View Scheme
参考文献
Bannister, Robin M.; Brookes, Michael H.; Evans, Graham R.; Katz, Ruth B.; Tyrrell, Nicholas D.
Organic Process Research and Development, 2000 , vol. 4, # 6 p. 467 - 472
