乙基4-氧代-4-(2,3,4-三甲氧基苯基)丁酸酯合成路线 (共 5 条)
反应条件
aluminium trichloride; nitrobenzene; tetrachloroethane, 1,1,2,2- T=-15°C; Erwaermen der mit Wasser gewaschenen Reaktionsloesung mit Aethanol und wenig Schwefelsaeure;
参考文献
Journal of the American Chemical Society, , vol. 67, p. 95,97
反应条件
tin(IV) chloride in dichloromethane
参考文献
Tetrahedron, , vol. 41, # 14 p. 2933 - 2938
反应条件
1: 8percent alcoholic alkali / 3 h / Heating 2: 86 percent / Zn amalgam, ccHCl, dimethyl sulphate / toluene; H2O / 48 h / Heating 3: 94 percent / polyphosphoric acid / 90 °C View Scheme
参考文献
Pelter, Andrew; Ward, Robert S.; Rao, Ramohan R.
Tetrahedron, 1985 , vol. 41, # 14 p. 2933 - 2938
参考文献
Pelter, Andrew; Ward, Robert S.; Rao, Ramohan R.
Tetrahedron, 1985 , vol. 41, # 14 p. 2933 - 2938
反应条件
1: 8percent alcoholic alkali / 3 h / Heating
2: 86 percent / Zn amalgam, ccHCl, dimethyl sulphate / toluene; H2O / 48 h / Heating
View Scheme
参考文献
Pelter, Andrew; Ward, Robert S.; Rao, Ramohan R.
Tetrahedron, 1985 , vol. 41, # 14 p. 2933 - 2938