1-(2-氯乙氧基)-2-硝基苯合成路线 （共 6 条）
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide) T=90°C; 2 h;
参考文献
MOLECULAR PROBES, INC.
Patent: WO2005/16874 A2, 2005 ;
Location in patent: Page/Page column 55 ;
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20°C; Mitsunobu reaction;
参考文献
Wyeth
Patent: US2007/37802 A1, 2007 ;
Location in patent: Page/Page column 61 ;
US 20070037802 A1
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20 - 140°C; 4 h;
参考文献
Cheng, Zhao; Yang, Bingqin; Yang, Meipan; Zhang, Binglin
Journal of the Brazilian Chemical Society, 2014 , vol. 25, # 1 p. 112 - 118
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 - 140 °C 2: iron; hydrogenchloride / ethanol / 4 h / |Reflux View Scheme
参考文献
Cheng, Zhao; Yang, Bingqin; Yang, Meipan; Zhang, Binglin
Journal of the Brazilian Chemical Society, 2014 , vol. 25, # 1 p. 112 - 118
反应条件
potassium carbonate
T=130°C; 16 h;
参考文献
Molecular Probes, Inc.
Patent: US7102005 B2, 2006 ;
Location in patent: Page/Page column 100 ;
US 7102005 B2
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide)
T=130°C; 18 h;
参考文献
MOLECULAR PROBES, INC.
Patent: WO2005/16874 A2, 2005 ;
Location in patent: Page/Page column 55-56 ;
