4-苯基-3-丁炔-1-醇合成路线 （共 39 条）
反应条件
2: 49 percent / n-Bu3SnH, AIBN / benzene / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 5 p. 641 - 644
Journal of Organic Chemistry, , vol. 57, # 25 p. 6803 - 6810
参考文献
Wessig, Pablo; Mueller, Gunnar
Chemical Communications, 2006 , # 43 p. 4524 - 4526
反应条件
1: 74 percent / phthalimide, PPh3, DIAD, H2NNH2 2: triphenylphosphine, hydrogen / rhodium(II) acetate dimer / ethyl acetate / 20 h / 80 - 90 °C View Scheme
参考文献
Campi; Chong; Jackson; Van Der Schoot
Tetrahedron, 1994 , vol. 50, # 8 p. 2533 - 2542
反应条件
hydrogen; Lindlar's catalyst
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 2, p. 1902 - 1905
Zhurnal Organicheskoi Khimii, , vol. 2, # 11 p. 1934 - 1938
反应条件
1: 86 percent / PPh3, HMPA, I2 / diethyl ether / 6 h / 0 °C 2: 1,4,8,11-tetramethyl-1,4,8,11-tetraazacyclotetradecanenickel(II) perchlorate, tetraethylammonium perchlorate / dimethylsulfoxide / Ambient temperature; constant current electrolysis View Scheme
参考文献
Ozaki; Mitoh; Ohmori
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 9 p. 1435 - 1440
反应条件
1: H2 / Pd-CaCO3 2: PBr3 View Scheme
参考文献
Cherkasov,L.N. et al.
Journal of Organic Chemistry USSR (English Translation), 1966 , vol. 2, p. 1902 - 1905
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, # 11 p. 1934 - 1938
反应条件
1: With [Ni0(1,5-cyclooctadiene)2]; diethylzinc; cesium fluoride in dimethyl sulfoxide; toluene T=50°C; 6 h; Inert atmosphere; 2: With hydrogenchloride in water
参考文献
Li, Suhua; Ma, Shengming
Chemistry - An Asian Journal, 2012 , vol. 7, # 10 p. 2411 - 2418
反应条件
1: 65 percent / pyridine / 1.) 1 h, room temp., 2.) 24 h, refrigerator 2: Na2CO3 / 288 h / 80 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 48, # 26 p. 5260 - 5268
反应条件
copper(l) iodide; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=100°C; Sonogashira reaction;
参考文献
Feuerstein, Marie; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2004 , vol. 45, # 8 p. 1603 - 1606
反应条件
copper(l) iodide; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=100°C; Sonogashira reaction;
参考文献
Feuerstein, Marie; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2004 , vol. 45, # 8 p. 1603 - 1606
