4-氰基-3-甲氧基苯甲酰氯合成路线 （共 3 条）
反应条件
thionyl chloride in toluene 3 h; Heating;
参考文献
Barraclough; Black; Cambridge; Demaine; Gerskowitch; Giles; Hill; Hull; Lyer; King; Livingstone; Nobbs; Randall; Shah; Whiting
Archiv der Pharmazie, 1990 , vol. 323, # 8 p. 507 - 512
反应条件
1: 1.) NaNO2, conc. HCl / 1.) H2O, 0-5 deg C, 1 h, 2.a) 50 deg C, 2.b) 2 h, reflux 2: SOCl2 / toluene / 3 h / Heating View Scheme
参考文献
Barraclough; Black; Cambridge; Demaine; Gerskowitch; Giles; Hill; Hull; Lyer; King; Livingstone; Nobbs; Randall; Shah; Whiting
Archiv der Pharmazie, 1990 , vol. 323, # 8 p. 507 - 512
反应条件
1.) THF, ether, 0-5 deg C, 1 h, 2.) dioxane, 2 h, reflux; Yield given. Multistep reaction;
参考文献
Barraclough; Black; Cambridge; Demaine; Gerskowitch; Giles; Hill; Hull; Lyer; King; Livingstone; Nobbs; Randall; Shah; Whiting
Archiv der Pharmazie, 1990 , vol. 323, # 8 p. 507 - 512
