2,3-二氢-3,3-二甲基-1,2-苯并异噻唑 1,1-二氧化物合成路线 （共 10 条）
反应条件
in tetrahydrofuran T=40°C; 3 h;
参考文献
Differding, Edmond; Lang, Robert W.
Helvetica Chimica Acta, 1989 , vol. 72, p. 1248 - 1252
反应条件
in tetrahydrofuran 3 h; UV-irradiation;
参考文献
Doepp, Dietrich; Lauterfeld, Peter; Schneider, Markus; Schneider, Dietmar; Henkel, Gerald; Issac, Yvette Abd el Sayed; Elghamry, Ibrahim
Synthesis, 2001 , # 8 p. 1228 - 1235
反应条件
in tetrahydrofuran T=-78°C; 2 h;
参考文献
Porter, Ned A.; Carter, Randall L.; Mero, Christopher L.; Roepel, Michael G.; Curran, Dennis P.
Tetrahedron, 1996 , vol. 52, # 12 p. 4181 - 4198
反应条件
T=600°C; P=0.001 Torr;
参考文献
Doepp, Dietrich; Krueger, Carl; Lauterfeld, Peter; Raabe, Eleonore
Angewandte Chemie, 1987 , vol. 99, # 2 p. 142 - 143
反应条件
1.1: t-BuLi / tetrahydrofuran; hexane / 1.25 h / -78 - 0 °C 1.2: 85 percent / tetrahydrofuran; hexane / 2 h / -78 °C 2.1: 95 percent / TMSCl; NaI / acetonitrile / 1 h / Heating View Scheme
参考文献
Liu, Zhaopeng; Shibata, Norio; Takeuchi, Yoshio
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 302 - 303
反应条件
1: 52 percent / tetrahydrofuran / 4 h / -78 °C 2: 31 percent / tetrahydrofuran / 2 h / -78 °C View Scheme
参考文献
Porter, Ned A.; Carter, Randall L.; Mero, Christopher L.; Roepel, Michael G.; Curran, Dennis P.
Tetrahedron, 1996 , vol. 52, # 12 p. 4181 - 4198
反应条件
hydrogenchloride; potassium iodide
参考文献
Doepp, Dietrich; Krueger, Carl; Lauterfeld, Peter; Raabe, Eleonore
Angewandte Chemie, 1987 , vol. 99, # 2 p. 142 - 143
反应条件
1-methoxy-2-phenylprop-1-enolate in tetrahydrofuran -78 deg C, 1 h, r.t., 1 h, other reagent; Product distribution;
参考文献
Differding, Edmond; Lang, Robert W.
Helvetica Chimica Acta, 1989 , vol. 72, p. 1248 - 1252
参考文献
Mustafa; Hilmy
Journal of the Chemical Society, 1952 , p. 1343
反应条件
NAF in chloroform Ambient temperature;
参考文献
Adcock, William; Binmore, Gavin T.; Krstic, Alexander R.; Walton, John C.; Wilkie, John
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2758 - 2766
