1,1′-硫代羰基二-2(1H)-吡啶酮合成路线 (共 18 条)
反应条件
in toluene T=110°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 51, # 13 p. 2613 - 2615
反应条件
ammonium cerium(IV) nitrate; iodine in acetonitrile T=50°C; Iodination; 24 h;
参考文献
Malamas, Michael S.; Sredy, Janet; Moxham, Christopher; Katz, Alan; Xu, Weixin; McDevitt, Robert; Adebayo, Folake O.; Sawicki, Diane R.; Seestaller, Laura; Sullivan, Donald; Taylor, Joseph R.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 7 p. 1293 - 1310
反应条件
in dichloromethane T=20°C; Substitution;
参考文献
European Journal of Organic Chemistry, , # 22 p. 3787 - 3792
反应条件
in toluene 1 h; Heating;
参考文献
Kim, Sunggak; Yi, Kyu Yang
Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2613 - 2615
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; thiocarbonylation; 0.5 h;
参考文献
Windhorst, Albert D.; Timmerman, Henk; Worthington, Edward A.; Bijloo, Greetje J.; Nederkoorn, Paul H. J.; Menge, Wiro M. P. B.; Leurs, Rob; Herscheid, Jacobus D. M.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 9 p. 1754 - 1761
反应条件
in dichloromethane 0.2 h; Ambient temperature;
参考文献
Kim, Sunggak; Yi, Kyu Yang
Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2613 - 2615
反应条件
in dichloromethane 0.5 h; Ambient temperature;
参考文献
Kim, Sunggak; Yi, Kyu Yang
Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2613 - 2615
反应条件
in dichloromethane 1 h; Ambient temperature;
参考文献
Kim, Sunggak; Yi, Kyu Yang
Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2613 - 2615
反应条件
in dichloromethane T=20°C;
参考文献
O'Connor, Stephen P.; Atwal, Karnail; Li, Chi; Liu, Eddie C.-K.; Seiler, Steven M.; Shi, Mengxiao; Shi, Yan; Stein, Philip D.; Wang, Ying
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 16 p. 4696 - 4699
反应条件
triethylamine in dichloromethane T=0 - 20°C; 0.333333 h;
参考文献
Digital Biotech Co., Ltd.
Patent: WO2004/35533 A1, 2004 ;
Location in patent: Page 38 ;
WO 2004/035533 A1