N,N’-二苯基-1,3-丙二胺合成路线 （共 13 条）
反应条件
sodium tetrahydroborate in ethanol
参考文献
Tetrahedron Letters, , vol. 39, # 47 p. 8645 - 8646
反应条件
1: With sodium sulfate in dichloromethane T=20°C; 18 h; 2: With sodium tetrahydroborate in ethanol T=0°C; 1 h;
参考文献
WO2008/27932 A2, ;
Page/Page column 109 ;
WO 2008/027932 A2
反应条件
in ethanol T=20°C; 56 h;
参考文献
Molecules, , vol. 7, # 4 p. 405 - 411
反应条件
1: MgSO4 / methanol / 1 h / Ambient temperature 2: NaBH4 / methanol / 2 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 34, # 3 p. 1032 - 1038
反应条件
in water 1.) 0 deg C to ambient temperature (slowly), 2.) reflux, overnight;
参考文献
Journal of Organic Chemistry, , vol. 56, # 17 p. 5063 - 5079
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 36 h; Heating; Yield given;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 6 p. 1027 - 1038
反应条件
1: NEt3 / CH2Cl2 / 0 °C 2: LiAlH4 / tetrahydrofuran / 36 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 6 p. 1027 - 1038
参考文献
Tetrahedron, , vol. 34, p. 371 - 378
反应条件
in THF-d8 (tetrahydrofuran-d8) 600 h; phosphate buffer in D2O; Equilibrium constantKinetics;
参考文献
European Journal of Organic Chemistry, , # 4 p. 681 - 695
反应条件
1: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O 2: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O 3: THF-d8 (tetrahydrofuran-d8) / 240 h / phosphate buffer in D2O View Scheme
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
