(1,4,7,10-四氮杂-环十二-1-基)-烯丙基乙酸酯合成路线 (共 3 条)
反应条件
in chloroform T=20°C; 6 h;
参考文献
Waengler; Eisenhut; Haberkorn; Mier
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 5 p. 2606 - 2616
反应条件
1: potassium carbonate / acetonitrile / 16 h / 20 °C 2: tetrakis(triphenylphosphine) palladium(0); 4-methyl-morpholine / dichloromethane / 2 h / 20 °C 3: tri-iso-propylsilane; trifluoroacetic acid; water / 3 h View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 50 p. 6810 - 6814
反应条件
1: potassium carbonate / acetonitrile / 16 h / 20 °C 2: tetrakis(triphenylphosphine) palladium(0); 4-methyl-morpholine / dichloromethane / 2 h / 20 °C View Scheme
参考文献
Jamous, Mazen; Haberkorn, Uwe; Mier, Walter
Tetrahedron Letters, 2012 , vol. 53, # 50 p. 6810 - 6814