4-甲基苯磺酸苯基甲基酯合成路线 （共 87 条）
反应条件
1: chlorosulphonic acid 2: aqueous acetone / Heating 3: 1.) Emmons procedure, 2.) acetonitrile, 50 deg C, 5 h View Scheme
参考文献
Yoh, Soo-Dong; Tsuno, Yuho; Fujio, Mizue; Sawada, Masami; Yukawa, Yasuhide
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 7 - 14
参考文献
Lee, Ikchoon; Lee, Won Heuy; Sohn, Se Chul; Kim, Choong Shik
Tetrahedron, 1985 , vol. 41, # 13 p. 2635 - 2642
反应条件
1.) Emmons procedure, 2.) acetonitrile, 50 deg C, 5 h; Multistep reaction;
参考文献
Yoh, Soo-Dong; Tsuno, Yuho; Fujio, Mizue; Sawada, Masami; Yukawa, Yasuhide
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 7 - 14
反应条件
2-fluoro-2-(piperidin-1-yl)-4-(2,3,5,6-tetrafluoropyridin-4-yl)-5-(2,4,6-triisopropylphenyl)-1,3-dithiole in 1,4-dioxane T=45°C; 10 h; Schlenk techniqueInert atmosphere;
参考文献
Ung, Gael; Bertrand, Guy
Chemistry--A European Journal, 2012 , vol. 18, # 41 p. 12955 - 12957,3
参考文献
Nodzu et al.
Yakugaku Zasshi, 1951 , vol. 71, p. 713
Chem.Abstr., 1952 , p. 3976
反应条件
1: benzyl p-toluenesulphonate With manganese in tetrahydrofuran T=20°C; Metallation; 0.5 h; 2: benzoyl chloride in tetrahydrofuran; ethylene dibromide T=20°C; Addition; 0.5 h;
参考文献
Kim, Seung-Hoi; Rieke, Reuben D.
Journal of Organic Chemistry, 2000 , vol. 65, # 8 p. 2322 - 2330
参考文献
Monatshefte fuer Chemie, , vol. 82, p. 588,592
反应条件
potassium carbonate in acetone Heating;
参考文献
Dewick, Paul M.
Synthetic Communications, 1981 , vol. 11, # 10 p. 853 - 858
反应条件
water in acetone T=25°C; Rate constant;
参考文献
Maskill, H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1241 - 1246
反应条件
water T=25°C; further ionic strength; Rate constantProduct distribution;
参考文献
Maskill, H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1241 - 1246
