2-氨基-1-甲基-3H-咪唑并[4,5-f]喹啉合成路线 (共 3 条)
反应条件
1: hydrogen / W2 Raney nickel / ethanol / 1 h 2: 1.8 g / ethanol / 3 h / Heating 3: 2.) potassium permanganate, 3.) sodium, ammonia, ferric chloride / 1.) toluene, reflux, 5 h, 2.) acetic acid, 25 deg C, 1.5 h, 3.) reflux, 8 h View Scheme
参考文献
Synthetic Communications, , vol. 18, # 9 p. 973 - 980
反应条件
1: 1.8 g / ethanol / 3 h / Heating 2: 2.) potassium permanganate, 3.) sodium, ammonia, ferric chloride / 1.) toluene, reflux, 5 h, 2.) acetic acid, 25 deg C, 1.5 h, 3.) reflux, 8 h View Scheme
参考文献
Synthetic Communications, , vol. 18, # 9 p. 973 - 980
反应条件
potassium permanganate; ammonia; sodium; iron(III) chloride 1.) toluene, reflux, 5 h, 2.) acetic acid, 25 deg C, 1.5 h, 3.) reflux, 8 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 18, # 9 p. 973 - 980