反应条件
in neat (no solvent) ampule with MoCl5 and Bi was heated to 230°C (2 h), to 350°C (2 h) and kept at 350°C for 12 h, cooled, homogenized and heated to 350°C (3 h) , reoriented and heated at 350°C for 24 h, cooled, treated with 12 M HCl; recrystn.; X-ray diffraction;
参考文献
Hay, Daniel N.T.; Adams, Juan A.; Carpenter, Jason; DeVries, Stephanie L.; Domyancich, John; Dumser, Bruce; Goldsmith, Shawn; Kruse, Melissa A.; Leone, Angela; Moussavi-Harami, Farid; O'Brien, Jennifer A.; Pfaffly, Jennifer R.; Sylves, Michael; Taravati, Parisa; Thomas, Jacob L.; Tiernan, Breck; Messerle, Louis
Inorganica Chimica Acta, 2004 , vol. 357, # 3 p. 644 - 648
