(1-氧代吡啶-1-鎓-2-基)甲醇合成路线 （共 9 条）
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform T=0°C; 0.5 h;
参考文献
Keizers, Peter H. J.; Saragliadis, Athanasios; Hiruma, Yoshitaka; Overhand, Mark; Ubbink, Marcellus
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14802 - 14812
反应条件
water; dihydrogen peroxide; acetic acid und Erwaermen des Reaktionsprodukts mit wss. Salzsaeure;
参考文献
Boekelheide; Linn
Journal of the American Chemical Society, 1954 , vol. 76, p. 1286,1289
反应条件
in acetonitrile MeN4Cl adding to the polarographic test soln. prepared from SnCl4*5H2O in acetonitrile containing a ligand in a molar ratio 2:1 and 1 M Pr4NClO4 as a supporting electrolyte under N2; detected polarographically;
参考文献
Drtil, A.; Meux, Jay; Meux, J. W.; Williams, R. J.; Rogers, J. W.
Polyhedron, 1983 , vol. 2, p. 479 - 484
反应条件
1: 1.) N,N-dimethylcarbamoyl chloride / 1.) CH2Cl2, a) RT, 90 min, b) reflux, 90 min, 2.) CH2Cl2, reflux, 36 h 2: 68 percent / aq. HF / acetonitrile View Scheme
参考文献
Bremberg, Ulf; Rahm, Fredrik; Moberg, Christina
Tetrahedron Asymmetry, 1998 , vol. 9, # 19 p. 3437 - 3443
反应条件
N,N-dimethylcarbamoyl chloride 1.) CH2Cl2, a) RT, 90 min, b) reflux, 90 min, 2.) CH2Cl2, reflux, 36 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bremberg, Ulf; Rahm, Fredrik; Moberg, Christina
Tetrahedron Asymmetry, 1998 , vol. 9, # 19 p. 3437 - 3443
反应条件
1,4-dioxane; selenium(IV) oxide T=90 - 100°C;
参考文献
Furukawa
Yakugaku Zasshi, 1958 , vol. 78, p. 957,959
Chem.Abstr., 1959 , p. 3219
反应条件
thionyl chloride in dichloromethane T=0°C; 2 h; Reflux;
参考文献
Keizers, Peter H. J.; Saragliadis, Athanasios; Hiruma, Yoshitaka; Overhand, Mark; Ubbink, Marcellus
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14802 - 14812
反应条件
1,4-dioxane; selenium(IV) oxide T=90 - 100°C;
参考文献
Furukawa
Yakugaku Zasshi, 1958 , vol. 78, p. 957,959
Chem.Abstr., 1959 , p. 3219
反应条件
selenium(IV) oxide in pyridine
4 h; Heating;
参考文献
Nienkemper, Katrin; Kehr, Gerald; Kehr, Seda; Froehlich, Roland; Erker, Gerhard
Journal of Organometallic Chemistry, 2008 , vol. 693, # 18 p. 3063 - 3073
