2-(3,4-二甲氧基苄基)哌啶合成路线 （共 7 条）
反应条件
hydrogen; platinum(IV) oxide in acetic acid T=20°C; P=1551.4 Torr; 10 h;
参考文献
Cardellini; Claudi; Perlini; Balduini; Cattabeni; Cimino
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 4 p. 307 - 317
反应条件
1: 84 percent / sodium hydride / toluene / 41 h / Heating 2: 1.) potassium hydroxide; 2.) 85percent H3PO4 / 1.) ethanol, water, 100 deg C; 2.) water, 115 deg C 3: 71 percent / hydrogen / PtO2 / acetic acid / 10 h / 20 °C / 1551.4 Torr View Scheme
参考文献
Cardellini; Claudi; Perlini; Balduini; Cattabeni; Cimino
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 4 p. 307 - 317
反应条件
1: 84 percent / sodium hydride / toluene / 41 h / Heating 2: 1.) potassium hydroxide; 2.) 85percent H3PO4 / 1.) ethanol, water, 100 deg C; 2.) water, 115 deg C 3: 71 percent / hydrogen / PtO2 / acetic acid / 10 h / 20 °C / 1551.4 Torr View Scheme
参考文献
Cardellini; Claudi; Perlini; Balduini; Cattabeni; Cimino
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 4 p. 307 - 317
反应条件
1: 1.) potassium hydroxide; 2.) 85percent H3PO4 / 1.) ethanol, water, 100 deg C; 2.) water, 115 deg C 2: 71 percent / hydrogen / PtO2 / acetic acid / 10 h / 20 °C / 1551.4 Torr View Scheme
参考文献
Cardellini; Claudi; Perlini; Balduini; Cattabeni; Cimino
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 4 p. 307 - 317
参考文献
Sugimoto
Yakugaku Zasshi, 1956 , vol. 76, p. 1045
Chem.Abstr., 1957 , p. 3598
反应条件
1: diethyl ether 2: zinc; hydrochloric acid; water 3: Raney nickel; dioxane / 150 °C / 60311.6 Torr / Hydrogenation View Scheme
参考文献
Sugimoto
Yakugaku Zasshi, 1956 , vol. 76, p. 1045
Chem.Abstr., 1957 , p. 3598
反应条件
1: diethyl ether 2: zinc; hydrochloric acid; water 3: Raney nickel; dioxane / 150 °C / 60311.6 Torr / Hydrogenation View Scheme
参考文献
Sugimoto
Yakugaku Zasshi, 1956 , vol. 76, p. 1045
Chem.Abstr., 1957 , p. 3598
