hydrogenchloride in 1,4-dioxane; water 24 h; Heating;

hydrogenchloride in 1,4-dioxane 10 h; Heating;

Multi-step reaction with 2 steps 1: 80 percent / LiClO4 / 45 °C / electrolysis at 0.06 A, 10 V2: 90 percent / H2 / 5percent Pd/C / ethyl acetate / 6 h / 760 Torr / Ambient temperature