3-(甲氧羰基)吡啶-5-硼酸频那醇酯合成路线 （共 3 条）
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in N,N-dimethyl-formamide T=0 - 80°C; 10 h;
参考文献
XCOVERY, INC.
Patent: WO2008/88881 A1, 2008 ;
Location in patent: Page/Page column 49 ;
WO 2008/088881 A1
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran T=80°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 2 p. 540 - 543
反应条件
1,10-phenanthroline; lithium hydroxide hydrate; CuTC in dichloromethane T=45°C; Inert atmosphere; regioselective reaction;
参考文献
Liu, Tianfei; Shao, Xinxin; Wu, Yaming; Shen, Qilong
Angewandte Chemie - International Edition, 2012 , vol. 51, # 2 p. 540 - 543
