1: sodium cyanoborohydride / CH2Cl2; methanol / 2 h / 0 °C
2: 30percent aq. hydrogen peroxide, sodium peroxide / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Bloodworth, A. J.; Courtneidge, J. L.; Curtis, Richard J.; Spencer, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2951 - 2955
1: sodium cyanoborohydride, toluene-p-sulphonic acid / tetrahydrofuran / 4 h / pH 3.5
2: 30percent aq. hydrogen peroxide, sodium peroxide / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Bloodworth, A. J.; Courtneidge, J. L.; Curtis, Richard J.; Spencer, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2951 - 2955
sodium peroxide; dihydrogen peroxide in tetrahydrofuran
24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Bloodworth, A. J.; Courtneidge, J. L.; Curtis, Richard J.; Spencer, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2951 - 2955
