4-(三氟甲硫基)苯基乙酸合成路线 (共 2 条)
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in hexane; cyclohexane T=-50°C; 24 h;
参考文献
Cabiddu; Cadoni; Corrias; Fattuoni; Floris; Melis
Journal of Organometallic Chemistry, 1997 , vol. 531, # 1-2 p. 125 - 140
反应条件
1: 86 percent / N,N-dimethylformamide / 20 h / 40 - 50 °C 2: 68 percent / 1.) 2 molar eq. sec-butyllithium, TMEDA / cyclohexane; hexane / 24 h / -50 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 531, # 1-2 p. 125 - 140