trichlorophosphate in chloroform 15 h; Heating;

<b>Multi-step reaction with 7 steps<br /> </b>1: 65 percent / H₂, conc. HCl / 10percent Pd/C / methanol / 760 Torr<br />2: 83 percent / 15 h / 90 &deg;C<br />3: 73 percent / POCl₃ / toluene / 15 h / 90 &deg;C<br />4: 85 percent / H₂, conc. HCl / 10percent Pd/C / ethanol / 4 h / 60 &deg;C / 2068.6 Torr<br />5: 95 percent / 1 N NaOH / ethanol / 3 h / Heating<br />6: SOCl₂ / 0.5 h / Heating<br />7: NH₃ (gas) / CH₂Cl₂ / 15 h<br /> <br /> &nbsp;

<b>Multi-step reaction with 4 steps<br /> </b>1: 85 percent / H₂, conc. HCl / 10percent Pd/C / ethanol / 4 h / 60 &deg;C / 2068.6 Torr<br />2: 95 percent / 1 N NaOH / ethanol / 3 h / Heating<br />3: SOCl₂ / 0.5 h / Heating<br />4: NH₃ (gas) / CH₂Cl₂ / 15 h<br /> <br /> &nbsp;

<b>Multi-step reaction with 5 steps<br /> </b>1: 73 percent / POCl₃ / toluene / 15 h / 90 &deg;C<br />2: 85 percent / H₂, conc. HCl / 10percent Pd/C / ethanol / 4 h / 60 &deg;C / 2068.6 Torr<br />3: 95 percent / 1 N NaOH / ethanol / 3 h / Heating<br />4: SOCl₂ / 0.5 h / Heating<br />5: NH₃ (gas) / CH₂Cl₂ / 15 h<br /> <br /> &nbsp;