双(二异丙基氨基)(2-氰基乙氧基)膦合成路线 （共 27 条）
反应条件
in tetrahydrofuran T=-10 - 20°C; 73.5 h;
参考文献
WO2003/106468 A1, ;
Page 6-7 ;
反应条件
1: diisopropylamine With phosphorus trichoride in acetonitrile 1 h; Inert atmosphere; 2: 3-hydroxy-propionitrile in hexane; acetonitrile 1.5 h; Inert atmosphere;
参考文献
Monatshefte fur Chemie, , vol. 141, # 7 p. 809 - 815
反应条件
triethylamine in diethyl ether Ambient temperature;
参考文献
Chemistry Letters, , p. 1401 - 1404
反应条件
1: 60 percent / phosphorus trichloride / diethyl ether / 12 h / Heating 2: triethylamine / diethyl ether / Ambient temperature View Scheme
参考文献
Chemistry Letters, , p. 1401 - 1404
反应条件
HEPES buffer; N-hexadecyl-N,N,N-trimethylammonium bromide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in hexane; pentan-1-ol T=25°C; variation of condition; Product distribution;
参考文献
Helvetica Chimica Acta, , vol. 76, # 3 p. 1341 - 1351
反应条件
pyridine 1.a) Et2O, -78 deg C, 1 h, 1.b) room temperature, 2.a) Et2O, -10 deg C, 1 h, 2.b) room temperature; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 46, # 2 p. 487 - 502
反应条件
N,N-diisopropylamine tetrazolide in acetonitrile 15 h;
参考文献
Kierzek, Ryszard; Rozek, Marek; Markiewicz, Wojciech T.
Bulletin of the Polish Academy of Sciences, Chemistry, 1987 , vol. 35, # 11-12 p. 507 - 516
反应条件
1H-tetrazole; diisopropylamine in dichloromethane
参考文献
Sudhakar Rao; Jayaraman; Durland; Revankar
Tetrahedron Letters, 1992 , vol. 33, # 50 p. 7651 - 7654
反应条件
1H-tetrazole in acetonitrile 2 h; Ambient temperature;
参考文献
Kumar, Anil; Katti, Seturam B.; Madhusudanan, Kunnath P.
Nucleosides and Nucleotides, 1997 , vol. 16, # 1-2 p. 11 - 22
反应条件
1H-tetrazole in acetonitrile T=20°C; 2 h;
参考文献
Charubala, Ramamurthy; Pfleidere, Wolfgang; Suhadolnik, Robert J.; Iacono, Kathryn T.; Muto, Nicholas F.; Homan, Joseph W.; Martinand-Mari, Camille; Horvath, Susan E.; Henderson, Earl E.; Steele, Amber; Rogers, Thomas J.
Helvetica Chimica Acta, 2002 , vol. 85, # 8 p. 2284 - 2299
