反应条件
1: 1.) BuLi / 1.) THF, 0 deg C, 2 h, 2.) THF, 0 deg C, 8 h; 0 to 20 deg C 2: TBAF, H2O / tetrahydrofuran 3: 1.) H5IO6, MeNH2, 2.) HCl, H2O / 1.) MeOH, H2O 4: Et3N / CH2Cl2 / 3 h 5: 75 percent / NaIO4, RuO2*H2O, H2O / acetonitrile; CCl4 / 2 h View Scheme
参考文献
Alvaro, Giuseppe; Martelli, Gianluca; Savoia, Diego; Zoffoli, Andrea
Synthesis, 1998 , # 12 p. 1773 - 1777
