乙基4-[乙氧基(氧代)乙酰基]苯甲酸酯合成路线 (共 4 条)
反应条件
pyridine; chromium(VI) oxide in dichloromethane 0.25 h;
参考文献
Creary, Xavier; Mehrsheikh-Mohammadi, M. E.
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2664 - 2668
反应条件
1: 95 percent / ZnI2 / 0.5 h / Ambient temperature 2: 59 percent / HCl / 16 h / Ambient temperature 3: 60 percent / CrO3, pyridine / CH2Cl2 / 0.25 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 14 p. 2664 - 2668
反应条件
1: 59 percent / HCl / 16 h / Ambient temperature 2: 60 percent / CrO3, pyridine / CH2Cl2 / 0.25 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 14 p. 2664 - 2668
反应条件
1: 4-iodobenzoic acid ethyl ester With phenyllithium in diethyl ether; cyclohexane T=-60°C; 1.13889E-05 h; Flow reactor; 2: oxalic acid diethyl ester in diethyl ether; cyclohexane T=-60°C; 0.000466667 h; Flow reactor; 3: With water; acetic acid in tetrahydrofuran; hexane Temperature;
参考文献
Nagaki, Aiichiro; Ichinari, Daisuke; Yoshida, Jun-Ichi
Chemical Communications, 2013 , vol. 49, # 31 p. 3242 - 3244