2-(4-溴苯基)-3-苯基咪唑并[1,2-a]吡啶合成路线 (共 4 条)
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water Suzuki Coupling; 24 h; Heating / reflux;
参考文献
Samsung SDI Co., Ltd.
Patent: EP1925618 A1, 2008 ;
Location in patent: Page/Page column 17 ;
反应条件
1: ethanol / 18 h / Reflux 2: N-iodo-succinimide / acetonitrile / 1 h / 20 °C 3: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 18 h / 80 °C View Scheme
参考文献
Samsung Mobile Display Co., Ltd.
Patent: EP2292601 A1, 2011 ;
反应条件
1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C 2: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 18 h / 80 °C View Scheme
参考文献
Samsung Mobile Display Co., Ltd.
Patent: EP2292601 A1, 2011 ;
反应条件
1: ethanol / 18 h / Reflux 2: N-iodo-succinimide / acetonitrile / 1 h / 20 °C 3: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 18 h / 80 °C View Scheme
参考文献
Samsung Mobile Display Co., Ltd.
Patent: EP2292601 A1, 2011 ;