反应条件
1: 1.) sodium nitrite, hydrobromic acid, 2.) cuprous bromide / 1.) 5 min, 2.) reflux
2: 1.) magnesium turnings, iodine, 2.) tellurium shot / 1.) THF, reflux, 0.5 h, 2.) reflux, 3 h
3: 1.) sodium borohydride / 1.) THF, ethanol, 2.) room temperature, 0.5 h
4: 96 percent / aq. potassium hydroxide / ethanol / 2 h / 50 °C
View Scheme
参考文献
Detty,M.R.; Murray,B.J.
Journal of the American Chemical Society, 1983 , vol. 105, p. 883
