反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '3572664', constants.ctx, '0')">trichloroacetic acid sodium salt</a>; <a href="#" onclick="return RXDsubstances(event, this, '507750', constants.ctx, '0')">β-naphthaldehyde</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=20°C; 0.666667 h; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '505999', constants.ctx, '0')">tert-butyldimethylsilyl chloride</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '103853', constants.ctx, '0')">1H-imidazole</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=20°C; 8 h; Further stages.; <br />
参考文献
Cafiero, Lauren R.; Snowden, Timothy S. Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2844 - 2847