1-methyl-pyrrolidin-2-one T=20 - 25°C; 24 h;

hydrogen sulfide in N,N-dimethyl-formamide 0.166667 h; Ambient temperature;

hydrogen sulfide in N,N-dimethyl-formamide 0.166667 h; Ambient temperature;

hydrogen sulfide in N,N-dimethyl-formamide 0.166667 h; Ambient temperature;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1879369', constants.ctx, '0')">[bis(acetoxy)iodo]benzene</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587194', constants.ctx, '0')">iodine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '506007', constants.ctx, '0')">acetic acid</a> <br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 0.015 g / diacetoxyiodobenzene, iodine / acetic acid / 0.17 h / 25 &deg;C<br />2: 0.008 g / Et₃N, acetic acid / acetone / 24 h / 20 - 25 &deg;C<br /> <br /> &nbsp;