2,2-二甲基-3-丁烯酸合成路线 (共 52 条)
反应条件
1: 72 percent / diethyl ether / 3 h / Heating 2: 60 percent / 6 M HCl / 18 h / Heating View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 406, # 1+2 p. 57 - 70
反应条件
in diphenylether T=200°C;
参考文献
Chemische Berichte, , vol. 102, p. 3922 - 3946
反应条件
n-butyllithium; diethylamine in tetrahydrofuran; hexane 1.) -78 deg C, 0.5 h, 2.) room temp., 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 54, # 17 p. 4357 - 4366
反应条件
1: sodium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / 12 h / 75 °C 2: lithium hydroxide hydrate; water / methanol View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 50, # 6 p. 1415 - 1418
参考文献
Journal of Organic Chemistry, , vol. 31, p. 1694 - 1698
反应条件
tetra-(n-butyl)ammonium iodide in N,N-dimethyl-formamide T=-10°C; Pt cathode, Mg anode, 25 mA/cm2; var. anode, temp.; Product distribution;
参考文献
Tetrahedron Letters, , vol. 36, # 19 p. 3345 - 3348
反应条件
1: HCl 2: (i) Mg, THF, (ii) /BRN= 1900390/, (iii) aq. HCl View Scheme
参考文献
Australian Journal of Chemistry, , vol. 28, p. 2535 - 2538
反应条件
ammonia; KNH2 anschliessend mit Methyljodid;
参考文献
Journal of the Chemical Society, , p. 1551,1554
反应条件
hydrogenchloride 18 h; Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 406, # 1+2 p. 57 - 70
反应条件
1: hydrogen chloride 2: phosphorus pentoxide; benzene 3: anschliessender Hydrolyse View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. <3>35, p. 121