反应条件
1: 1,3-cylohexanedione With methylhydrazine in tetrahydrofuran; methanol T=0°C; 1.5 h; 2: N,N-dimethyl-formamide dimethyl acetal in tetrahydrofuran; methanol T=20 - 120°C; 0.166667 h; Microwave irradiation;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; TREU, Matthias
Patent: WO2012/10704 A1, 2012 ;
Location in patent: Page/Page column 51 ;
WO 2012/010704 A1