2-(1-甲基乙烯基)苯酚合成路线 (共 27 条)
反应条件
1: Methyltriphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran T=20°C; Wittig Olefination; 2 h; 2: o-hydroxyacetophenone in tetrahydrofuran T=-78 - 30°C; Wittig Olefination;
参考文献
Konishi, Hideyuki; Muto, Takashi; Manabe, Kei; Ueda, Tsuyoshi
Organic Letters, 2012 , vol. 14, # 18 p. 4722 - 4725,4
反应条件
in tetrahydrofuran; diethyl ether T=-78°C; 0.416667 h;
参考文献
Jones; Van De Water; Lindsey; Hoarau; Ung; Pettus
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3435 - 3441
参考文献
Journal of the Chemical Society, , p. 1774,1785
Journal of the American Chemical Society, , vol. 55, p. 284,291, 293
Journal of the American Chemical Society, , vol. 53, p. 3390,3394
参考文献
Journal of the Chemical Society, , p. 1774,1785
Journal of the American Chemical Society, , vol. 55, p. 284,291, 293
参考文献
Journal of the Chemical Society, , p. 1774,1785
Journal of the American Chemical Society, , vol. 55, p. 4151
反应条件
2: sulfuric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 55, p. 284,291, 293
反应条件
1: 88 percent / NaH / tetrahydrofuran / 4 h / 20 °C 2: 57 percent / tetrahydrofuran; diethyl ether / 0.42 h / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 10 p. 3435 - 3441
反应条件
1: diethyl ether 2: 150 °C / 300 Torr View Scheme
参考文献
Helvetica Chimica Acta, , vol. 60, # 6 p. 2007 - 2033
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 20, p. 1561 - 1570