N-(4-氰基苯基)苯甲酰胺合成路线 （共 21 条）
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran
T=45°C; Arylation; 19 h;
参考文献
Yin, Jingjun; Buchwald, Stephen L.
Organic Letters, 2000 , vol. 2, # 8 p. 1101 - 1104
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran
T=45°C; 18 h;
参考文献
Yin, Jingjun; Buchwald, Stephen L.
Journal of the American Chemical Society, 2002 , vol. 124, # 21 p. 6043 - 6048
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
T=25°C; 2 h;
参考文献
Sasaki, Kaname; Crich, David
Organic Letters, 2011 , vol. 13, # 9 p. 2256 - 2259
反应条件
1: benzoic acid With 1-methyl-piperidine; isopropyloxycarbonylchloride in tetrahydrofuran; toluene
T=0°C; 0.333333 h;
2: With LiAlHSeH in tetrahydrofuran; toluene
T=0 - 5°C; 0.5 h;
3: 4-Cyanophenyl azide in tetrahydrofuran; toluene
T=25°C;
参考文献
Wu, Xinghua; Hu, Longqin
Journal of Organic Chemistry, 2007 , vol. 72, # 3 p. 765 - 774
反应条件
piperidine; N-ethyl-N,N-diisopropylamine in acetonitrile
T=25°C; 1 h;
参考文献
Surabhi, Prathima; Wu, Xinghua; Hu, Longqin
Tetrahedron Letters, 2006 , vol. 47, # 27 p. 4609 - 4613
反应条件
tetrabutylammomium bromide in 1-methyl-pyrrolidin-2-one; dimethyl sulfoxide; N,N-dimethyl-formamide
T=100°C; Air;
参考文献
Inamoto, Kiyofumi; Shiraishi, Mitsugu; Hiroya, Kou; Doi, Takayuki
Synthesis, 2010 , # 18 p. 3087 - 3090
反应条件
pyridine hydrochloride in acetonitrile
T=40°C; 8 h; Inert atmosphere;
参考文献
Heller, Stephen T.; Fu, Tingting; Sarpong, Richmond
Organic Letters, 2012 , vol. 14, # 8 p. 1970 - 1973
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; tri-cyclo-hexyl-phosphine in toluene
T=110°C; 12 h;
参考文献
Nakaya, Ryotaro; Yorimitsu, Hideki; Oshima, Koichiro
Chemistry Letters, 2011 , vol. 40, # 9 p. 904 - 906
反应条件
oxygen; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=120°C; 2 h;
参考文献
Inamoto, Kiyofumi; Hasegawa, Chisa; Kawasaki, Junpei; Hiroya, Kou; Doi, Takayuki
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2643 - 2655
反应条件
in dimethyl sulfoxide; ethyl acetate
T=5 - 20°C; 0.5 h;
参考文献
Wu, Xinghua; Hu, Longqin
Tetrahedron Letters, 2005 , vol. 46, # 48 p. 8401 - 8405
