1,1,1,2,2,3,3,5,5,5-十氟-4-碘-4-(三氟甲基)戊烷合成路线 （共 13 条）
反应条件
potassium fluoride; iodine; silver trifluoroacetate 1.) acetonitrile, room temperature, 1 h, 30 deg C, 30 min; 2.) room temperature, 1 h, reflux, 2.5 h; Yield given. Multistep reaction;
参考文献
Probst, A.; Raab, K.; Ulm, K.; Werner, K. von
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 223 - 246
反应条件
T=40°C; Irradiationquartz reactor;
参考文献
Probst, A.; Raab, K.; Ulm, K.; Werner, K. von
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 223 - 246
反应条件
T=40°C; Irradiationquartz reactor;
参考文献
Probst, A.; Raab, K.; Ulm, K.; Werner, K. von
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 223 - 246
反应条件
lithium bromide in acetonitrile T=0°C; 0.25 h; also with LiI and LiCl, variation of time; Product distributionMechanism;
参考文献
Blume, Elisabeth; Gasafi-Martin, Waltraud; Probst, Anton; Werner, Konrad von
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 387 - 396
参考文献
Rozhkov, I. N.; Igumnov, S. M.; Pletnev, S. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 1.2 p. 209
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 1 p. 226 - 227
反应条件
zinc in acetic anhydride 3 h; Ambient temperature; Product distribution;
参考文献
Blume, Elisabeth; Gasafi-Martin, Waltraud; Probst, Anton; Werner, Konrad von
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 387 - 396
反应条件
in various solvent(s) T=0 - 5°C; 70 h;
参考文献
Rozhkov, I. N.; Igumnov, S. M.; Pletnev, S. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 1.2 p. 209
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 1 p. 226 - 227
反应条件
lithium bromide in acetonitrile T=0°C; 0.25 h; also with LiI and LiCl, variation of time; Product distributionMechanism;
参考文献
Blume, Elisabeth; Gasafi-Martin, Waltraud; Probst, Anton; Werner, Konrad von
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 387 - 396
反应条件
in ethyl acetate T=80 - 90°C; 6 h; Heating;
参考文献
Pletnev, S. I.; Igumnov, S. M.; Rozhkov, I. N.; Rempel', G. D.; Ponomarev, V I.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 2 p. 1892 - 1895
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 9, p. 2057 - 2061
反应条件
1-hexene; zinc in ethyl acetate T=80°C; Yield given. Yields of byproduct given;
参考文献
Igumnov, S. M.; Rozhkov, I. N.; Pletnev, S. I.; Borisov, Yu. A.; Rempel', G. D.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 10 p. 2122 - 2125
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 10 p. 2308 - 2312
