4-(4-甲基-1H-咪唑-1-基)苯胺合成路线 (共 2 条)
反应条件
ammonium formate; palladium 10 on activated carbon in ethanol; water T=2°C; 2 h; Reflux;
参考文献
Demont, Emmanuel Hubert; Garton, Neil Stuart; Gosmini, Romain Luc Marie; Hayhow, Thomas George Christopher; Seal, Jonathan; Wilson, David Matthew; Woodrow, Michael David
Patent: US2012/208798 A1, 2012 ;
Location in patent: Page/Page column 44 ;
反应条件
1: potassium carbonate / acetonitrile / 70 h / 60 °C / Inert atmosphere 2: ammonium formate / palladium 10 on activated carbon / ethanol / 2 h / Reflux; Inert atmosphere View Scheme