1: phenyl-magnesium bromide With ZnI2(tmeda) in tetrahydrofuran
2: p-toluenesulfonic acid 1-methyl-heptyl ester With anhydrous iron chloride in tetrahydrofuran
T=0 - 25°C;
chloro-trimethyl-silane; bismuth(III) chloride in neat (no solvent)
T=50°C; 2 h; Title compound not separated from byproducts;
参考文献
Labrouillere, Mireille; Roux, Christophe Le; Oussaid, Abdelouahad; Gaspard-Iloughmane, Hafida; Dubac, Jacques
Bulletin de la Societe Chimique de France, 1995 , vol. 132, p. 522 - 530
