6-辛基-3,4-二氢萘-2(1h)-酮合成路线 (共 2 条)
反应条件
1: oct-1-ene With 9-bora-bicyclo[3.3.1]nonane in tetrahydrofuran T=20°C; 2: 6-bromo-1,2,3,4-tetrahydronaphthalen-2-one With sodium hydroxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water 12 h; Heating / reflux; Product distribution / selectivity;
参考文献
UNIVERSITY OF VIRGINIA PATENT FOUNDATION
Patent: WO2008/64315 A1, 2008 ;
Location in patent: Page/Page column 37 ;
WO 2008/064315 A1
反应条件
1: oct-1-ene With 9-bora-bicyclo[3.3.1]nonane in water 2: C11H9F3O4S With potassium phosphate; potassium bromide; tetrakis(triphenylphosphine) palladium(0) in water T=65°C; 2 h; Product distribution / selectivity;
参考文献
UNIVERSITY OF VIRGINIA PATENT FOUNDATION
Patent: WO2008/64315 A1, 2008 ;
Location in patent: Page/Page column 52 ;
WO 2008/064315 A1