N-丙-2-烯基苯甲酰胺合成路线 （共 65 条）
反应条件
1: 91 percent / LDA / tetrahydrofuran; hexane / -70 deg C, 10 min, then to 0 deg C 2: 1.) sec-butyllithium / 1.) THF, cyclohexane, -70 deg C, 10 min 2.) THF, to 0 deg C View Scheme
参考文献
Fisher, Lawrence E.; Muchowski, Joseph M.; Clark, Robin D.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2700 - 2705
反应条件
(i) NaH, (ii) /BRN= 507487/, (iii) Pd(OAc)2, Cu(OAc)2, LiCl; Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 24, p. 1992 - 1999
反应条件
1: N2O4, AcOK / 1,2-dimethoxy-ethane / -10 °C 2: CaCO3 / dioxane / 85 - 110 °C View Scheme
参考文献
Heterocycles, , vol. 30, # 2 p. 789 - 793
反应条件
potassium meta-periodate; [{Ru(η3:η3-C10H16)(μ-Cl)Cl}2] in water T=100°C; 3 h;
参考文献
Cadierno, Victorio; Gimeno, Jose; Nebra, Noel
Chemistry - A European Journal, 2007 , vol. 13, # 23 p. 6590 - 6594
反应条件
di-tert-butyl peroxide; hypophosphorous acid in 1,4-dioxane 18 h; Heating;
参考文献
Synthesis, , # 1-2 p. 63 - 68
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Zhang, Tongxin; Zhang, Yan; Zhang, Weixi; Luo, Meiming
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2775 - 2780
反应条件
oxygen; cobalt(II) 2,4-pentanedionate in isopropyl alcohol T=75°C; 1 h;
参考文献
Kato; Yamada; Takai; Inoki; Isayama
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 1 p. 179 - 186
反应条件
hydrogen fluoride; SbF5 T=-20°C; 0.166667 h;
参考文献
Thibaudeau, Sebastien; Martin-Mingot, Agnes; Jouannetaud, Marie-Paule; Karam, Omar; Zunino, Fabien
Chemical Communications, 2007 , # 30 p. 3198 - 3200
反应条件
oxygen; isopropyl alcohol; bis(trifluoroacetylacetonato)cobalt(II) T=75°C; 4 h;
参考文献
Isayama, Shigeru; Mukaiyama, Teruaki
Chemistry Letters, 1989 , p. 569 - 572
反应条件
sulfuric acid; sulfur trioxide T=90°C;
参考文献
Engman, Lars
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3425 - 3430
