N-丙-2-烯基苯甲酰胺合成路线 (共 65 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; palladium diacetate in 1,4-dioxane
T=125°C; 0.166667 h; microwave irradation;
参考文献
Appukkuttan, Prasad; Axelsson, Linda; der Eycken, Erik Van; Larhed, Mats
Tetrahedron Letters, 2008 , vol. 49, # 39 p. 5625 - 5628
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; [(t-Bu)3PH]BF4; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in 1,4-dioxane
T=160°C; 0.333333 h; microwave irradiation;
参考文献
Appukkuttan, Prasad; Axelsson, Linda; der Eycken, Erik Van; Larhed, Mats
Tetrahedron Letters, 2008 , vol. 49, # 39 p. 5625 - 5628
反应条件
potassium hydroxide; aluminum oxide in 1,4-dioxane
T=40°C; 8 h;
参考文献
Sukata, Kazuaki
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 3 p. 838 - 843
反应条件
pyridine; water; methyllithium in diethyl ether; hexane
参考文献
Beak, Peter; Basha, Anwer; Kokko, Bruce; Loo, DeKai
Journal of the American Chemical Society, 1986 , vol. 108, # 19 p. 6016 - 6023
反应条件
[Cu(μ-OH)(tmeda)]2Cl2; caesium carbonate in acetonitrile
T=20°C; 5 h;
参考文献
Kumaraswamy; Pitchaiah; Ramakrishna; Sadaiah
Tetrahedron Letters, 2006 , vol. 47, # 12 p. 2013 - 2015
反应条件
N,O-bis-(trimethylsilyl)-acetamide in tetrahydrofuran
T=20°C; 3 h;
参考文献
Wu, Wenting; Zhang, Zhihui; Liebeskind, Lanny S.
Journal of the American Chemical Society, 2011 , vol. 133, # 36 p. 14256 - 14259
反应条件
hydrogenchloride in tetrahydrofuran
Ambient temperature;
参考文献
DeBruin, Kenneth E.; Boros, Eric E.
Journal of Organic Chemistry, 1990 , vol. 55, # 25 p. 6091 - 6098
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile
T=0°C;
参考文献
Taniguchi, Takahiko; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4679 - 4682
反应条件
1: allyl-magnesium chloride With indium(III) chloride in tetrahydrofuran
T=20°C; Inert atmosphere;
2: azidobenzoic acid in benzene
3 h; Photolysis;
3: With water; sodium hydroxide in benzene
参考文献
Bencivenni, Giorgio; Lanza, Tommaso; Minozzi, Matteo; Nanni, Daniele; Spagnolo, Piero; Zanardi, Giuseppe
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 15 p. 3444 - 3450
反应条件
bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=60°C; 1 h;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 9 p. 2721 - 2722