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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
102834-26-4
合成路线
（共 8 条）
102834-26-4
→
反应条件
498-02-2
4'-羟基-3'-甲氧基苯乙酮
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C 3: RuH2(CO)(PPh3)3; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; hydrogen / deuterated toluene / 20 h / 135 °C / 760.05 Torr View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
102834-26-4
→
反应条件
22317-35-7
+
498-02-2
4'-羟基-3'-甲氧基苯乙酮
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; water / 16 h / 20 °C 3: Ru(H)2(CO)(PPh3)(xantphos) / deuterated toluene / 20 h / 135 °C / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
102834-26-4
→
反应条件
22317-35-7
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
102834-26-4
→
反应条件
22317-35-7
+
498-02-2
4'-羟基-3'-甲氧基苯乙酮
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; water / 16 h / 20 °C 3: Ru(H)2(CO)(PPh3)(xantphos) / deuterated toluene / 20 h / 135 °C / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
102834-26-4
→
反应条件
7382-59-4
愈创木酚基甘油-Β-愈创木基丙醚
反应条件
1: N,N-dimethyl-formamide / 26.84 °C 2: potassium carbonate; sodium hydroxide / dimethyl sulfoxide / 26.84 °C 3: sodium tetrahydroborate / ethanol / 26.84 °C View Scheme
参考文献
Badamali, Sushanta K.; Luque, Rafael; Clark, James H.; Breeden, Simon W.
Catalysis Communications, 2011 , vol. 12, # 11 p. 993 - 995
102834-26-4
→
反应条件
22317-34-6
反应条件
1: N,N-dimethyl-formamide / 26.84 °C 2: potassium carbonate; sodium hydroxide / dimethyl sulfoxide / 26.84 °C View Scheme
参考文献
Badamali, Sushanta K.; Luque, Rafael; Clark, James H.; Breeden, Simon W.
Catalysis Communications, 2011 , vol. 12, # 11 p. 993 - 995
98-88-4
苯甲酰氯
→
反应条件
102834-26-4
反应条件
Multi-step reaction with 2 steps 1: pyridine / 4.84 °C2: bromine / chloroform / -0.16 °C
参考文献
Badamali, Sushanta K.; Luque, Rafael; Clark, James H.; Breeden, Simon W. Catalysis Communications, 2011 , vol. 12, # 11 p. 993 - 995
1252675-90-3
→
反应条件
102834-26-4
反应条件
Multi-step reaction with 3 steps 1.1: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C2.1: RuH2(CO)(PPh3)3; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; hydrogen / deuterated toluene / 20 h / 135 °C / 760.05 Torr3.1: pyridine / chloroform / 1 h / 20 °C3.2: 16 h / 20 °C
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R. Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
