N-(3-丁烯-1-基)-4-甲基苯磺酰胺合成路线 (共 23 条)
反应条件
potassium carbonate in acetone
T=60°C; Inert atmosphere;
参考文献
Belmessieri, Dorine; Cordes, David B.; Slawin, Alexandra M. Z.; Smith, Andrew D.
Organic Letters, 2013 , vol. 15, # 13 p. 3472 - 3475
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 3 h; Inert atmosphere;
参考文献
Combettes, Lorraine E.; Schuler, Marie; Patel, Rakesh; Bonillo, Baltasar; Odell, Barbara; Thompson, Amber L.; Claridge, Tim D. W.; Gouverneur, Veronique
Chemistry - A European Journal, 2012 , vol. 18, # 41 p. 13126 - 13132
反应条件
triethylamine in dichloromethane
T=0 - 20°C;
参考文献
Couty, Sylvain; Barbazanges, Marion; Meyer, Christophe; Cossy, Janine
Synlett, 2005 , # 6 art. no. G48504ST, p. 905 - 910
反应条件
copper(ll) bromide in dimethyl sulfoxide
T=100°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Tang, Xiaodong; Huang, Liangbin; Qi, Chaorong; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemical Communications, 2013 , vol. 49, # 54 p. 6102 - 6104
反应条件
1: PPh3; DEAD / tetrahydrofuran / 0 - 20 °C
2: K2CO3 / methanol / 3 h / Heating
View Scheme
参考文献
Marion, Frederic; Coulomb, Julien; Servais, Aurore; Courillon, Christine; Fensterbank, Louis; Malacria, Max
Tetrahedron, 2006 , vol. 62, # 16 p. 3856 - 3871
反应条件
potassium carbonate in acetone
参考文献
Handa, Sandeep; Kachala, Manpreet S.; Lowe, Sarah R.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 253 - 256
反应条件
potassium carbonate in acetone
7 h; Heating;
参考文献
Wang, Yuanyuan; Wang, Jingxin; Su, Jiachun; Huang, Feng; Jiao, Lei; Liang, Yong; Yang, Dazhi; Zhang, Shiwei; Wender, Paul A.; Yu, Zhi-Xiang
Journal of the American Chemical Society, 2007 , vol. 129, # 33 p. 10060 - 10061
反应条件
hydrogenchloride in methanol; water
参考文献
Wucherpfennig,W.
Justus Liebigs Annalen der Chemie, 1971 , vol. 746, p. 16 - 27
反应条件
tri-n-butyl-tin hydride
参考文献
Rigby, James H.; Danca, Diana M.; Horner, John H.
Tetrahedron Letters, 1998 , vol. 39, # 46 p. 8413 - 8416
反应条件
sodium hydride in N,N-dimethyl-formamide
17 h; Heating;
参考文献
Cheng, Hsiu-Yi; Sun, Chong-Si; Hou, Duen-Ren
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2674 - 2677