1,2-二溴-3-甲基丁烷合成路线 （共 24 条）
反应条件
bromine in chloroform T=-65°C;
参考文献
Mori, Kenji; Horinaka, Akio; Kido, Masaru
Liebigs Annalen der Chemie, 1994 , # 8 p. 817 - 826
反应条件
1: 1.) LiAlH4, AlCl3, 2.) lithium powder / 1.) ether, THF, -60 deg C, 2 h, 2.) -60 deg C, 8 h 2: Br2 / CCl4 View Scheme
参考文献
Barluenga, Jose; Yus, Miguel; Concellon, Jose M.; Bernad, Pablo
Journal of Organic Chemistry, 1981 , vol. 46, # 13 p. 2721 - 2726
反应条件
1: 5,6,8,9-tetrahydro-7-phenyldibenzo<c,h>xanthenylium tetrafluoroborate / CH2Cl2 / 400 h / 20 °C 2: bromine, 2-methylbut-2-ene, MeCH2(Me)C=CH2 / CHCl3; CH2Cl2 / -12 °C View Scheme
参考文献
Katritzky, Alan R.; Lloyd, Jeremy M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2347 - 2352
反应条件
1: quinoline hydrobromide; quinoline / 130 - 135 °C 2: hydrobromic acid 3: hydrobromic acid View Scheme
参考文献
Kutscherow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1913 , vol. 45, p. 1653
Chem. Zentralbl., 1914 , vol. 85, # I p. 754
反应条件
1: hydrobromic acid 2: hydrobromic acid View Scheme
参考文献
Kutscherow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1913 , vol. 45, p. 1653
Chem. Zentralbl., 1914 , vol. 85, # I p. 754
参考文献
Kutscherow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1913 , vol. 45, p. 1653
Chem. Zentralbl., 1914 , vol. 85, # I p. 754
反应条件
Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Yus, Miguel; Concellon, Jose M.; Bernad, Pablo
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 3116 - 3118
反应条件
T=180 - 185°C; daneben entstehen Monobrom- und Tribromsubstitutionsprodukte des 2-Methylbutans;
参考文献
Faworsdi
Justus Liebigs Annalen der Chemie, 1907 , vol. 354, p. 362
Chem. Zentralbl., 1908 , vol. 79, # I p. 1041
参考文献
Kutscherow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1913 , vol. 45, p. 1653
Chem. Zentralbl., 1914 , vol. 85, # I p. 754
参考文献
Ipatjew
Chem. Zentralbl., 1898 , vol. 69, # II p. 472
