Gerrard, W.; Mooney, E. F.; Rees, R. G.
Journal of the Chemical Society, 1964 , p. 740 - 745
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.5.4.4, page 104 - 106
in toluene under N2; soln. of BBr3 (1.05 equiv) in toluene added dropwise at -78 °C to suspn. of (CuMes)5*toluene in toluene; mixt. stirred at -78 °C for 2 h and then allowed to slowly warm to room temp. overnight; after filtration all volatiles removed under high vac.; crude product purified by distn. under reduced pressure; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 681, # 1-2 p. 134 - 142
in toluene under N2; soln. of BBr3 (0.48 equiv) in toluene added dropwise at -78 °C to suspn. of (CuMes)5*toluene in toluene; mixt. allowed to slowly warm to room temp.; mixt. heated to 100 °C for 12 h; after filtration all volatiles removed under high vac.; crude product purified by recrystn. from hexanes at -37 °C; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 681, # 1-2 p. 134 - 142
