反应条件
n-BuLi in hexane (N2); addn. of n-BuLi in hexane to C6BrF5 in light petroleum at -78°C, stirring (1 h), addn. of BBr3 in light petroleum at -78°C, further stirring (room temp., 15 h); filtration (Celite), concn., decantation, drying (vac.), further purifn.by vac. sublimation (140°C, E-1 Torr);
参考文献
Chernega, Alexander N.; Graham, Andrew J.; Green, Malcolm L. H.; Haggitt, Jane; Lloyd, Julian; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1997 , # 13 p. 2293 - 2304
