McCusker, P. A.; Bright, H. H.
Journal of Inorganic and Nuclear Chemistry, 1966 , vol. 28, p. 2261 - 2266
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Gmelin Handbook: B: B-Verb.9, 6.3.2, page 303 - 314
in further solvent(s) further solvent: BBr3; at or below room temp. with rise in heat;;
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Gmelin Handbook: Nb: MVol.B1, 89, page 190 - 192
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in hexane byproducts: Me3SiBr, EtBBr2; addn. of soln. of BBr3 to soln. of Et3B3N3H2(SiMe3) (inert atmosphere, -30°C), mixt. warmed to room temp. (stirring, ca 1 h); volatiles evapd. (vac.); oily residue distd.: forerun (40-45°C/1 Torr, ca 20percent) of essentially pure BrEt2B3N3H3; main fraction (66-73°C/1 Torr, ca 60percent) of mixt. of some BrEt2B3N3H3 and mostly BrEt2B3N3H2SiMe3; residue: Et3B3N3H2(Et2B3N3H3);
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Niedenzu, Kurt; Serwatowska, Joanne; Serwatowski, Janusz
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 5 p. 713 - 717
in 1,2,5-trimethyl-benzene byproducts: (Br2B2Se3); from a mixture of BBr3 and (C8H14B)2Se in mesitylene a solid is precipitated (composed B2Br2Se3), the solvent is removed and oily C8H14BBr is obtained; for by-product: elem. anal., MS, mp = 325°C (dec.);
in toluene dropping BBr3 to soln. of bis-9-borabicyclo(3,3,1)nonane at 80-120°C, stirring at 100°C for 30 min; evapn.;
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Koester, R.; Grassberger, M. A.
Liebigs Annalen der Chemie, 1968 , vol. 719, p. 169 - 186
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Gmelin Handbook: B: B-Verb.9, 6.3.2, page 303 - 314
