Mikhailov, B. M.; Kozminskaya, T. K.
Bull. Acad. Sci. USSR Div. Chem. Sci., 1959 , p. 1785 - 1786
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Gmelin Handbook: B: B-Verb.9, 5.3.2, page 233 - 238
in chlorobenzene
adding dropwise Al(CH3)3 to stirred soln. of BBr3 in C6H5Cl at -70°C; slow heating while stirring at <=20°C until completion of exothermic react.; stirring at room temp. for two h; vac.distn.;
参考文献
Willcockson, G. W.
Patent: US3083228 , 1963 ;
C.A., 1963 , vol. 59, p. 8788
in acetone
under CO2 or N2, yield depending on molar ratio of educts;
参考文献
Noeth, H.; Fritz, P.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1963 , vol. 322, p. 297 - 309
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Paetzold, P. I.; Hansen, H.-J.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1966 , vol. 345, p. 79 - 86
