反应条件
in benzene
anhydrous and oxygen-free condns., BBr3 in benzene dropped into a soln. of B-compd. in benzene at 0°C with stirring, after 1 h allowed to attain ambient temp. within 30 min; removal of benzene, distn. ((Me2N)2BBr), dissolved in hexane, cooled to -78°C for 9 days, filtered; elem. anal.;
参考文献
Linti, Gerald; Loderer, Dirk; Noeth, Heinrich; Polborn, Kurt; Rattay, Wilfried
Chemische Berichte, 1994 , vol. 127, # 10 p. 1909 - 1922
