1: boron tribromide; trimethylsilyl ethylene in dichloromethane T=20°C; 13 h; 2: MIDA in dichloromethane; dimethyl sulfoxide T=23°C; 0.0833333 h;
参考文献
Burke, Martin D.; Gillis, Eric P.; Lee, Suk Joong; Knapp, David M.; Gray, Kaitlyn C.
Patent: US2009/30238 A1, 2009 ;
Location in patent: Page/Page column 23 ;
Irradiation (UV/VIS); hydrolysis of intermediate dibromide;
参考文献
Bowie,R.A.; Musgrave,O.C.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 566 - 571
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Gmelin Handbook: B: B-Verb.9, 5.3.3, page 238 - 244
Joannis
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 139, p. 364
Full Text Show Details
Gmelin Handbook: B: MVol., 7.4, page 112 - 112
2,2'-azo-bisisobutyronitrile react. at 0 °C, then warming to 20 °C, 20 h stirring at 80 °C; saponification of intermediate dibromide;
参考文献
Gmelin Handbook: B: B-Verb.9, 5.3.3, page 238 - 244
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Hoffmann, A. K.; Groszos, St. J.
Patent: US2882317 , 1959 ;
C.A., 1959 , p. 16062
Ashby, E. C.; Foster, W. E.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3407 - 3408
Full Text View citing articles Show Details
Gmelin Handbook: B: B-Verb.14, 3.8.1.2.1, page 94 - 97
